Details
Export Top Purity 2-amino-2',5-dichlorobenzophenone oxime 13949-49-0 In Stock
- Molecular Formula: C13H10 Cl2 N2 O
- Molecular Weight: 281.141
- Boiling Point: 464.4°Cat760mmHg
- Flash Point: 234.7°C
- PSA： 58.61000
- Density: 1.38g/cm3
- LogP: 4.38340
13949-49-0 Relevant articles
2-Benzazepines. 8. Zerovalent nickel mediated biaryl synthesis of an anxiolytic pyrimido[5,4-d][2]benzazepine
Coffen,Schaer,Bizzarro,Cheung
, p. 296 - 300 (2007/10/02)
-
13949-49-0 Process route
-
-
76049-50-8
2',5-dichloro-2-iodobenzophenone
-
-
13949-49-0
2',5-Dichloro-2-aminobenzophenone oxime
| Conditions | Yield |
|---|---|
|
With
piperidine; hydroxylamine hydrochloride;
In
pyridine;
for 20h;
Heating;
|
27.4%
|
-
-
2958-36-3,53960-29-5
(2-amino-5-chloro-phenyl)-(2-chloro-phenyl)-methanone
-
-
13949-49-0
2',5-Dichloro-2-aminobenzophenone oxime
| Conditions | Yield |
|---|---|
|
Multi-step reaction
with
2
steps
1: 1) NaNO2
/HCl/aq. CH3
COOH, 2) aq. KI
2: 27.4 percent / NH2
OH*HCl, piperidine / pyridine / 20 h / Heating
With
piperidine; hydrogenchloride; hydroxylamine hydrochloride; acetic acid; potassium iodide; sodium nitrite;
In
pyridine;
|
|
|
Multi-step reaction
with
2
steps
1: 1) NaNO2
/HCl, 2) KI/I2
/ 1) aq. CH3
COOH, 0.5 h, below 20 deg C, 2) 2.5 h, 5-10 deg C
2: 27.4 percent / NH2
OH*HCl, piperidine / pyridine / 20 h / Heating
With
piperidine; hydrogenchloride; hydroxylamine hydrochloride; iodine; potassium iodide; sodium nitrite;
In
pyridine;
|
13949-49-0 Upstream products
-
76049-50-8
2',5-dichloro-2-iodobenzophenone
-
2958-36-3
(2-amino-5-chloro-phenyl)-(2-chloro-phenyl)-methanone
13949-49-0 Downstream products
-
87999-67-5
6-Chloro-4-(o-chlorophenyl)-1,2,3-benzotriazine 3-Oxide
-
87999-68-6
2',5-Dichloro-2-iodobenzophenone (E)-Oxime
-
87999-69-7
2,3'-Dichlorobenzophenone (Z)-Oxime
Relative Products
- 4-(1-PHENETHYL-3-PHENYL-PROPYL)-PYRIDINE
- 2-[2-(2-chloro-1,1,2-trifluoroethoxy)phenyl]-5-[[4-(hexadecylsulphonyl)phenyl]amino]-2,4-dihydro-4-[[4-(2-phenoxyethoxy)phenyl]azo]-3H-pyrazol-3-one
- ANILINE D5
- 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,12,12,13,13,14,14,15,15,16,17,17,17-octacosafluoro-2-hydroxy-16-(trifluoromethyl)heptadecyl acrylate
- 2-(dimethoxyphosphinyl)ethyl laurate
- 2-[2-(dimethylamino)-1-[(dimethylamino)methyl]ethoxy]ethanol
- 1-(2,5-disulphophenyl)-4,5-dihydro-5-oxo-1H-pyrazole-3-carboxylic acid
- 2-[4-[(2-chloro-4-nitrophenyl)azo]-4,5-dihydro-3-methyl-5-oxo-1H-pyrazol-1-yl]ethyl (3,4-dichlorophenyl)carbamate
- 4-[(4-aminophenyl)sulphonyl]phenol
- ()-1-(isopropylamino)-3-(naphthyloxy)propan-2-ol
- (1S)-2-Oxobornane-10-sulphonic acid, compound with 1-(3,4-dimethoxybenzyl)-6,7-dimethoxyisoquinoline (1:1)
- 2,6-Dimethyl-4-phenylpyrylium hexafluoroarsenate
- trans-4'-ethyl-2-fluoro-4-(4-pentylcyclohexyl)-1,1'-biphenyl
- 3-[(4,5-dihydro-3-methyl-5-oxo-1-phenyl-1H-pyrazol-4-yl)azo]-N-[4-[[1-[2-[4-(hexadecyloxy)phenyl]-4-methyl-3,6-dioxocyclohexa-1,4-dien-1-yl]ethyl]sulphonyl]phenyl]-4-methoxybenzenesulphonamide
- (butylstannylidyne)tris(thioethane-1,2-diyl) tris[(9Z,12Z)-octadeca-9,12-dienoate]
- 7-hydroxy-8-[[4'-[(4-hydroxyphenyl)azo]-3,3'-dimethyl[1,1'-biphenyl]-4-yl]azo]naphthalene-1,3-disulphonic acid
- 3-Bromofuran
- TETRAPHENYLBIPHOSPHINE
- 2-ethyl-1-(2,4,6-trimethylbenzoyl)-1H-imidazole
- Carbenoxolone