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Manufacturer supply good quality SODIUM THIOPHENOXIDE 930-69-8 with stock
- Molecular Formula: C6H6S.Na
- Molecular Weight: 132.161
- Vapor Pressure: 2.07mmHg at 25°C
- Melting Point: >300 °C
- Boiling Point: 169.1°C at 760mmHg
- Flash Point: 50.6°C
- PSA: 25.30000
- Density: 1.079g/cm3
- LogP: 2.24300
SODIUM THIOPHENOXIDE(Cas 930-69-8) Usage
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Preparation |
Sodium thiophenolate is prepared by the following steps:A solution of (11) ( 1.0 g, 2.8 mmol), phenylthiol (0.33 g, 3.0 mmol), acetonitrile ?(5 cm3) and sodium carbonate (0.3 g) was stirred under reflux for 19 h. Water (20 cm3) ?was added, then the mixture extracted into DCM. The DCM solution was dried (MgS04) ?and evaporated to dryness. Chromatography on silica gel with DCM - hexane (30 : 70) as ?the eluent yielded 2,6-dibromo-3,5-difluoro-4-thiophenoxypyridine (0.9 g, 85%), m.p.65.5-66.5 OC (Found: C, 34.45; H, 1.3; N, 3.2. C11H5Bf2F2NS requires C, 34.7; H, ?1.3; N, 3.7%); IR spectrum no. 16; mass spectrum no. 19; nmr spectrum no. 16. |
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General Description |
Sodium thiophenolate can be prepared from the reaction of sodium and thiophenol in diethyl ether. |
InChI:InChI=1/C6H6S.Na/c7-6-4-2-1-3-5-6;/h1-5,7H;/q;+1/p-1
930-69-8 Relevant articles
Geometrically unprecedented 3-, 5- and 7-membered Hg(II)-Cu(I) and Hg(II)-Ag(I) thiolate clusters: Precursors to intermetallics
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, p. 8932 - 8937 (2015)
The syntheses of three polynuclear heter...
The influence of thiolate ligands on the luminescence properties of cycloplatinated(II) complexes
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, p. 15919 - 15927 (2017)
Complexes [Pt(C^N)(PPh3)Cl] (C^N = bzq (...
A single, low, oral dose of a 5-carbon-linked trioxane dimer orthoester plus mefloquine cures malaria-infected mice
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, p. 2773 - 2775 (2011)
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The nucleophilic reactivities of substit...
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The kinetics of the ring-opening reactio...
930-69-8 Process route
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108-98-5
thiophenol
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930-69-8
sodium thiophenolate
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882-33-7
diphenyldisulfane
| Conditions | Yield |
|---|---|
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With
sodium hydroxide;
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5535-49-9
2-Chloroethyl phenyl sulfide
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108-88-3,15644-74-3,16713-13-6
toluene
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-
74-85-1
ethene
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-
622-20-8
1,2-bis(phenylthio)ethane
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-
930-69-8
sodium thiophenolate
| Conditions | Yield |
|---|---|
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930-69-8 Upstream products
-
3019-20-3
isopropylthiobenzene
-
108-98-5
thiophenol
-
882-33-7
diphenyldisulfane
-
5510-78-1
diphenylthiophosphinic acid-S-phenyl ester
930-69-8 Downstream products
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62049-82-5
2,4-bis(phenylthio)nitrobenzene
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14710-97-5
(5-chloro-2,4-dinitro-phenyl)-phenyl sulfide
-
79236-84-3
1,5-dinitro-2,4-bis(phenylsulfanyl)benzene
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860241-51-6
4-benzenesulfonyl-1-nitro-2-phenylsulfanyl-benzene
Relative Products
- 3-[(4,5-dihydro-3-methyl-5-oxo-1-phenyl-1H-pyrazol-4-yl)azo]-N-[4-[[1-[2-[4-(hexadecyloxy)phenyl]-4-methyl-3,6-dioxocyclohexa-1,4-dien-1-yl]ethyl]sulphonyl]phenyl]-4-methoxybenzenesulphonamide
- (butylstannylidyne)tris(thioethane-1,2-diyl) tris[(9Z,12Z)-octadeca-9,12-dienoate]
- 7-hydroxy-8-[[4'-[(4-hydroxyphenyl)azo]-3,3'-dimethyl[1,1'-biphenyl]-4-yl]azo]naphthalene-1,3-disulphonic acid
- 3-Bromofuran
- TETRAPHENYLBIPHOSPHINE
- 2-ethyl-1-(2,4,6-trimethylbenzoyl)-1H-imidazole
- Carbenoxolone
- 2-AMINO-4-IMINO-2-THIAZOLINE HYDROCHLORIDE
- Propyltriphenylphosphonium bromide
- 4-(1,1,3,3-tetramethylbutyl)pyrocatechol
- 4,5-Dihydro-5-(4-fluorophenyl)-2(3H)-furanone
- ALLOCRYPTOPINE
- 2-Bromo-1-tetralone
- [[(diethylamino)thioxomethyl]thio]acetic acid
- 2-Bromophenol
- [[(aminocarbonyl)amino]carbonyl]oxamide
- disodium 1-[2-(carboxymethoxy)ethyl]-1-(carboxymethyl)-4,5-dihydro-2-undecyl-1H-imidazolium chloride
- 2-CYANOETHYLMETHYLDIETHOXYSILANE
- ALUMINUM DI(SEC-BUTOXIDE)ACETOACETIC ESTER CHELATE
- 1-[2-[(2-chlorophenyl)amino]ethyl]-4-methylpyridinium chloride