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SODIUM THIOPHENOXIDE

Basic Information

  • CAS No.: 930-69-8
  • Purity: 99%
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Details

Manufacturer supply good quality SODIUM THIOPHENOXIDE 930-69-8 with stock

  • Molecular Formula: C6H6S.Na
  • Molecular Weight: 132.161
  • Vapor Pressure: 2.07mmHg at 25°C 
  • Melting Point: >300 °C 
  • Boiling Point: 169.1°C at 760mmHg 
  • Flash Point: 50.6°C 
  • PSA: 25.30000 
  • Density: 1.079g/cm3 
  • LogP: 2.24300 

SODIUM THIOPHENOXIDE(Cas 930-69-8) Usage

Preparation

Sodium thiophenolate is prepared by the following steps:A solution of (11) ( 1.0 g, 2.8 mmol), phenylthiol (0.33 g, 3.0 mmol), acetonitrile ?(5 cm3) and sodium carbonate (0.3 g) was stirred under reflux for 19 h. Water (20 cm3) ?was added, then the mixture extracted into DCM. The DCM solution was dried (MgS04) ?and evaporated to dryness. Chromatography on silica gel with DCM - hexane (30 : 70) as ?the eluent yielded 2,6-dibromo-3,5-difluoro-4-thiophenoxypyridine (0.9 g, 85%), m.p.65.5-66.5 OC (Found: C, 34.45; H, 1.3; N, 3.2. C11H5Bf2F2NS requires C, 34.7; H, ?1.3; N, 3.7%); IR spectrum no. 16; mass spectrum no. 19; nmr spectrum no. 16.

General Description

Sodium thiophenolate can be prepared from the reaction of sodium and thiophenol in diethyl ether.

InChI:InChI=1/C6H6S.Na/c7-6-4-2-1-3-5-6;/h1-5,7H;/q;+1/p-1

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930-69-8 Process route

thiophenol
108-98-5

thiophenol

sodium thiophenolate
930-69-8

sodium thiophenolate

diphenyldisulfane
882-33-7

diphenyldisulfane

Conditions
Conditions Yield
With sodium hydroxide;
2-Chloroethyl phenyl sulfide
5535-49-9

2-Chloroethyl phenyl sulfide

toluene
108-88-3,15644-74-3,16713-13-6

toluene

ethene
74-85-1

ethene

1,2-bis(phenylthio)ethane
622-20-8

1,2-bis(phenylthio)ethane

sodium thiophenolate
930-69-8

sodium thiophenolate

Conditions
Conditions Yield

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