Details
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1.What is the ANILINE D5 ?
Aniline-d5 is intended for use as an internal standard for the quantification of Aniline by GC- or LC-mass spectrometry.
-
-
4165-57-5
bromobenzene-d5
-
-
4165-61-1
aniline-d5
| Conditions | Yield |
|---|---|
|
bromobenzene-d5;
With
copper(l) iodide; potassium carbonate; 4R-4-hydroxyproline;
In
dimethyl sulfoxide;
With
ammonium hydroxide;
In
dimethyl sulfoxide;
at 80 ℃;
|
61.1%
|
|
With
ammonium hydroxide; copper(l) iodide; potassium carbonate; 4R-4-hydroxyproline;
In
dimethyl sulfoxide;
at 80 ℃;
|
61.1%
|
|
With
ammonium hydroxide; copper(l) iodide; potassium carbonate; 4R-4-hydroxyproline;
In
dimethyl sulfoxide;
at 80 ℃;
|
61.1%
|
|
With
ammonium hydroxide; copper(l) iodide; potassium carbonate; 4R-4-hydroxyproline;
In
dimethyl sulfoxide;
at 80 ℃;
|
61.1%
|
|
With
copper(l) iodide; ammonia; potassium carbonate; 4R-4-hydroxyproline;
In
water; dimethyl sulfoxide;
at 80 ℃;
|
61.1%
|
|
With
iron(III) chloride; iron(III) oxide; ammonia;
In
water;
at 60 ℃;
for 19h;
Temperature;
|
45.3%
|
|
With
copper(I) oxide; ammonium hydroxide;
In
1-methyl-pyrrolidin-2-one;
at 80 ℃;
for 15h;
|
|
|
With
copper(I) oxide; ammonium hydroxide;
In
1-methyl-pyrrolidin-2-one; water;
at 80 ℃;
for 16h;
Sealed tube;
|
|
|
With
copper(I) oxide; ammonia;
In
1-methyl-pyrrolidin-2-one; water;
at 80 ℃;
for 15h;
|
|
|
With
copper(I) oxide; ammonia; oxygen;
In
1-methyl-pyrrolidin-2-one; water;
at 80 ℃;
|
|
|
With
copper(I) oxide; ammonium hydroxide;
In
1-methyl-pyrrolidin-2-one;
at 80 ℃;
|
-
-
4165-60-0
nitrobenzene-d5
-
-
4165-61-1
aniline-d5
| Conditions | Yield |
|---|---|
|
With
palladium 10% on activated carbon; ammonium formate;
In
methanol;
for 0.333333h;
Inert atmosphere;
Reflux;
|
98.3%
|
|
With
iron; ammonium chloride;
In
water;
at 100 ℃;
for 4h;
|
97%
|
|
With
palladium on activated charcoal; hydrogen;
In
methanol;
at 20 ℃;
for 16h;
under 2280.15 Torr;
Autoclave;
|
92%
|
|
With
hydrogenchloride; iron;
In
water;
|
91%
|
|
With
palladium on activated charcoal; hydrogen;
In
methanol;
at 20 ℃;
for 24h;
under 2585.81 Torr;
|
82%
|
|
With
palladium on activated charcoal; hydrogen;
In
methanol;
at 20 ℃;
for 24h;
under 2585.81 Torr;
|
81%
|
|
nitrobenzene-d5;
With
acetic acid;
In
ethanol;
for 0.166667h;
Reflux;
With
iron(III) chloride hexahydrate; iron;
for 4h;
Reflux;
|
80%
|
|
With
iron; calcium chloride;
In
ethanol; water;
at 60 ℃;
Sonication;
|
79.5%
|
|
With
palladium 10% on activated carbon; hydrogen;
In
methanol;
at 20 ℃;
for 12h;
under 3102.97 Torr;
|
78%
|
|
With
hydrogenchloride; tin;
for 1h;
Heating;
|
73%
|
|
nitrobenzene-d5;
With
acetic acid; zinc;
for 1h;
Reflux;
With
sodium carbonate;
In
water;
|
67%
|
|
With
palladium 10% on activated carbon; hydrogen;
In
methanol;
at 20 ℃;
under 760.051 Torr;
|
|
|
With
palladium 10% on activated carbon; hydrogen;
In
methanol;
at 20 ℃;
under 760.051 Torr;
Inert atmosphere;
|
|
|
With
iron; ammonium chloride;
In
ethanol; water;
at 110 ℃;
|
|
|
With
hydrogenchloride; tin;
In
water;
|
|
|
With
hydrogenchloride; tin;
In
ethanol;
at 20 ℃;
for 6h;
|
|
|
With
iron; ammonium chloride;
In
ethanol; water;
at 110 ℃;
for 2h;
|
|
|
With
hydrogenchloride; iron;
In
methanol; water;
at 70 ℃;
for 0.75h;
Inert atmosphere;
|
|
|
With
palladium on activated charcoal; hydrogen;
|
|
|
With
palladium on activated charcoal; hydrogen;
|
|
|
With
iron; ammonium chloride;
In
water;
at 100 ℃;
for 4h;
|
2.What is the CAS number for ANILINE D5 ?
The CAS number of ANILINE D5 is 4165-61-1.
More information of ANILINE D5 4165-61-1 are:
|
CAS?Number |
4165-61-1 |
|
Density |
1.076 g/mL at 25 °C |
|
Melting Point |
-6oC(lit.) |
|
Boiling Point |
184 °C(lit.) |
|
Flash Point |
158 °F |
|
Vapor Pressure |
0.7 mm Hg ( 25 °C) |
|
Refractive Index |
n20/D 1.5836(lit.) |
|
HS CODE |
2845901000 |
|
PSA |
26.02000 |
|
LogP |
1.85000 |
3.What are another words for ANILINE D5 ?
Synonyms?for?ANILINE D5 4165-61-1:Phenyl-d5-amine;Benzen-d5-amine;Aniline-2,3,4,5,6-d5;2,3,4,5,6-pentadeuterio-aniline;Aniline-d5;
4.What is the molecular formula of ANILINE D5?
The chemical formula of ?ANILINE D5 is?C6H7N which containing 6 Carbon atoms,7 Hydrogen atoms and 1 Nitrogen atoms,and the molecular weight of??ANILINE D5?is 98.0886.
5.What is ANILINE D5 (4165-61-1) used for?
Aniline D5, also known as perdeuterated aniline, is a chemical compound with the formula C6D5NH2, where the hydrogen atoms are replaced by deuterium atoms. It is a colorless, oily liquid that is used as a solvent and a reagent in various chemical reactions. Aniline D5 is particularly useful in nuclear magnetic resonance (NMR) spectroscopy due to its ability to provide a clear and distinct signal, which helps in the identification and characterization of other compounds in a mixture. It is also employed in the synthesis of deuterated compounds for research purposes, as well as in the pharmaceutical and chemical industries for the production of deuterated drugs and other specialty chemicals.
InChI:InChI=1/C6H7N/c7-6-4-2-1-3-5-6/h1-5H,7H2/i1D,2D,3D,4D,5D
Relevant articles related to ANILINE D5:
|
Article |
Source |
|
Scalable and selective deuteration of (hetero)arenes |
Bartling, Stephan,Beller, Matthias,Bourriquen, Florian,Brückner, Angelika,Junge, Kathrin,Kreyenschulte, Carsten,Lei, Aiwen,Li, Wu,Lund, Henrik,Rabeah, Jabor,Rockstroh, Nils,Surkus, Annette-Enrica,Yang, Dali , (2022/01/19) |
|
Benzocarbazole Synthesis via Visible-Light-Accelerated Rh(III)-Catalyzed C-H Annulation of Aromatic Amines with Bicyclic Alkenes |
Wang, Yichun,Jia, Deyang,Zeng, Jing,Liu, Yuming,Bu, Xiubin,Yang, Xiaobo supporting information, p. 7740 - 7745 (2021/10/20) |
6.Buy ANILINE D5 with the best price .
Chuanggao New Bio-Technical Material Co., Ltd is a quality supplier of ANILINE D5. Our main goal is customer satisfaction. Contact us to negotiate the best price for your business on ANILINE D5 4165-61-1.
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